Several issues are highlighted, including the usefulness of incorporating residual indent shape in the comparisons, as well as loaddisplacementtime data, and the signi. Measuring, evaluating, and describing pileup and sink in during nanoindentation of thin films on substrates by marianne sullivan a dissertation submitted to the graduate faculty of auburn university in partial fulfillment of the requirements for the degree of doctor of philosophy auburn, al december 12, 2015 keywords. Hardness and elastic modulus of micromaterials can be evaluated by analyzing instrumented sharptipindentation loaddepth curves. Pileup sink in of ratesensitive nanoindentation creeping solids. Uncertainties and errors in nanoindentation 55 load. Some modification of the oliver and pharr method by intrducing nw parameters have also been reported11, 12. Pileup and sinkin nanoindentation behaviors in alcocrfeni. Experimental tests have been conducted on nanocrystalline nc, ultrafinegrained ufg, and coarsegrained cg copper samples with a new berkvoich indenter at the strain rate of 0. For analysis of the indentation face, multiaxis flip stages are on the market. Published 5 october 2007 2007 iop publishing ltd modelling and simulation in materials. With contributions from leading researchers in the field, this book is divided into three parts. On the use of nanoindentation for cementitious materials g. Measuring, evaluating, and describing pileup and sinkin during.
Nanoindentation hardness measurement in piling up sio2 coating. Pileup or sinkin is always a concern in a nanoindentation test because it gives rise to errors in the estimation of the projected contact area when it is theoretically. Pileup and sinkin nanoindenta tion behaviors in alcocrfeni multiphase high entropy alloy. An expanding cavity model incorporating pileup and sink. Extensive progress has been made in the last 20 years in refining the instrumentation of nanoindentation. Bull chemical engineering and advanced materials newcastle university newcastle upon tyne ne1 7ru, uk abstract during nanoindentation testing there are many issues that need to be considered if high. Description of general pileup pattern as outlined in the introduction, the anisotropy associated with nanoindentation of a single crystal in different crystallographic orientations has been intensively studied recently due to the fact that the pileup and sink in patterns are significantly different than in the case of isotropic materials. Indentation is perhaps the most commonly applied means of testing the mechanical properties of materials.
Overall, this research contributes a number of new findings of pileup and sink in related to plasticity, and improves the field of nanoindentation as this new information can be utilized for the most accurate extraction of material properties from simple smallscale nanoindentation tests. The reason for the pileup and sink in is attributed to the dislocation activity in the individual crystal structure. Pileup sink in of ratesensitive nanoindentation creeping solids 825 cheng and cheng 1998 used a scaling approach to study pileup and sink in of rateinsensitive elasticplastic solids in the presence of work hardening caused by indentation. Pileup correction of mechanical characteristics of. Experiments have shown that nanoindentation unloading curves obtained with berkovich triangular pyramidal indenters are usually welldescribed by the powerlaw relation p. An investigation of nanomechanical properties of materials. The important factors in this technique are the force calibration and the depth, or socalled. Yangtse and chemin 1998 simulated a 3d frictionless rigid conical indenter tip indenting. Download product flyer is to download pdf in new tab. Habrakena a argenco department, university of liege, chemin des chevreuils 1, 4000 liege, belgium. Journal of materials research, cambridge university press cup, 2012, 27, pp. Then the sample is precisely positioned under the nanoindenter to perform a mechanical analysis on the same location. Bull chemical engineering and advanced materials newcastle university newcastle upon tyne ne1 7ru, uk abstract during nanoindentation. We present a study about the dependence of nanoindentation pileup patterns and of microtextures on the crystallographic orientation using high purity copper single crystals.
It is possible to measure the pileup contact area using computerized image analysis of atomic force microscope afm images of the indentations. Overall, this research contributes a number of new findings of pileup and sink in related to plasticity, and improves the field of nanoindentation as this new information can be utilized for the most accurate extraction of material properties from simple smallscale nanoindentation. Published 5 october 2007 2007 iop publishing ltd modelling and simulation in materials science and engineering, volume 15, number 7. A numerical study on the nanoindentation response of a. For the proposed ecm, it is assumed that the volume of material displaced by the indenter is equal to the volume loss, due to elastic deformation, in the material and depends on the pileup or sink. The multiple phases present in the alcocrfeni high entropy alloy are the reasons behind the different nanoindentation. Measurement of hardness and elastic modulus by instrumented. In this work, a finite element model was used to evaluate the pile up effect on the determination of mechanical properties from spherical indentation in a wide range of elastic. Pdf finite element analysis of spherical indentation to. In a last step, this location can again be moved under the afm to characterize and understand stressinduced features such as material pileup, sink. On the use of nanoindentation for cementitious materials. Pdf a comparison of nanoindentation pileup in bulk materials. Substrate effect and nanoindentation fracture toughness based.
Next, we have measured pileup and sink in with a technique. Pileupsinkin of ratesensitive nanoindentation creeping. Measuring, evaluating, and describing pileup and sinkin. However, depending on the substrate material, the behaviour can vary at the maximum indentation depth, as illustrated in fig. Pileups and sinkins influence the measurement of the contact area in indentation. First, we show our model is an improved method to the nanoindentation technique, and is vital in testing films on substrates. Nanoindentationinduced pileup in the residual impression. The occurrence of such pileup and sinkin patterns is usually interpreted in terms of the strainhardening behavior of the indented material 14. Experiments were conducted on a hysitron nanoindentation. A comparison of nanoindentation pile up in bulk materials and thin films n.
Pileups and sinkins influence the measurement of the contact area in indentation hardness testing particularly when the indent size becomes significantly small, i. Description of general pileup pattern as outlined in the introduction, the anisotropy associated with nanoindentation of a single crystal in different crystallographic orientations has been intensively studied recently due to the fact that the pileup and sink. Correction of the hardness measurement for pileup materials with a. Knowledge of the true hardness of the film can be used to assess the effects of the elastic modulus mismatch on the nanoindentation. An expanding cavity model incorporating pileup and sinkin. Relationship of stiffnessbased indentation properties using. Determination of mechanical properties by nanoindentation. Interests and limitations of nanoindentation for bulk. Finite element analysis of spherical indentation to study pileup sink in phenomena in steels and experimental validation. The present study quantified the effects of tipblunting and pileup or sink in on the contact area by analyzing indentation curves. Nanoindentation, also called intrumented indentation testing, is a variety of indentation hardness tests applied to small volumes. Nanoindentation morphologies of crystalline copper have been probed at the grain scale. Nanoindentation hardness measurement in piling up sio2. Analysis of sharptipindentation loaddepth curve for.
Instrumented indentation enables the determination of parameters for characterization of viscoelastic response. Nanoindentation has developed as a practical tool for determining the mechanical properties of thin. Atkins a g et al 1966 indentation hardness and creep of solids institute of metals journal part 11 94 36978. Use of quasistatic nanoindentation data to obtain stress. Round robin into best practices for the determination of. A comparison of nanoindentation pileup in bulk materials and thin films n. This study proposes an improved methodology to calculate the real mechanical characteristics of individual phases in various steels with significant pile up. This is a short video illustration to help you understand nanoindentation method for materials local mechanical properties measurement, mainly on elastic modulus and. Pileup is often found in some ductile soft materials including bulks and thin films. The possible causes of pile up and sink in phenomena during nanoindentation test are strain rate sensitivity and work hardening influence. Materials with large yield strengthtoyoungs modulus ratio, ye, are likely to show sink in upon nanoindentation loading, while materials with small ye can show either sink in or pileup, depending on the. Applied nanoindentation in advanced materials solid. The multiple phases present in the alcocrfeni high entropy alloy are the reasons behind the different nanoindentation behaviors, which were identified using electron microscopy. The pileup or sinkin effects can be observed in the indentation test, which depends on the strain hardening coefficient of the target material.
Pileup sink in of ratesensitive nanoindentation creeping solids 825 cheng and cheng 1998 used a scaling approach to study pileup and sink in of rateinsensitive elasticplastic solids in. Evaluating pileup and sinkin during nanoindentation of thin. A numerical study on pileup in nanoindentation creep. Orientation dependent nanoindentation orientation dependent nanoindentation of alphatitanium. Depth dependence of nanoindentation pileup patterns in copper single crystals stanislaw kucharski and dariusz jarza. We are interested in a better understanding of the deformation zone around nanoindents and indents. Evaluating pileup and sinkin during nanoindentation of. Correcting for contact area changes in nanoindentation using. An investigation of nanomechanical properties of materials using nanoindentation and artificial neural network skip to main content thank you for visiting. The oliver and pharr method however is not efficent eneough when pile up or sink in occurs in the specimen. Ebsd, rotation, pattern, pileup, sinkin, modeling, cpfem. Pdf hardness is a characteristic of a material, not a fundamental physical property.
Request pdf a numerical study on pileup in nanoindentation creep in this paper, we simulate materials of variable hardness, work hardening exponent. The effects of pileup, viscoelasticity and hydrostatic. Applied nanoindentation in advanced materials addresses this need and is a comprehensive, selfcontained reference covering applied aspects of nanoindentation in advanced materials. Nanoindentation behavior of high entropy alloys with. Nanoindentation pileup viscoelasticity hydrostatic stress abstract. Sink in patterns reduce and pileup patterns increase the contact area. The nanoindentation process on druckerprager type materials has been modelled by fem and the results compared to experimental results obtained in a range of polymer. Crystals free fulltext nanoindentationinduced pileup. Jan 01, 2008 read a numerical study on pile up in nanoindentation creep, international journal of surface science and engineering on deepdyve, the largest online rental service for scholarly research with thousands of academic publications available at your fingertips. Not taking the pilingup or sinkingin into account in micro and nanoindentation hardness tests can result in errors when extracting hardness or related. Problems associated with the pileup or sink in of the material on the edges of the indent during the indentation process remain a problem that is still under investigation. A new expanding cavity model ecm for describing conical indentation of elasticideally plastic material is developed.
Investigation of the mechanical properties of thin films. A numerical study on the nanoindentation response of a particle embedded in a matrix teck fei low b mechatronics eng hons thesis submitted in accordance with the requirements for. Nanoindentation under dynamic conditions ii abstract nanoindentation has emerged as a leading technique for the investigation of mechanical properties on small volumes of material. Van vliet massachusetts institute of technology, cambridge, ma 029, usa abstract recent. Next, we have measured pileup and sink in with a technique including scanning electron microscopy images to better understand the effects of these phenomena on material properties. Nanoindentation the indentation itself is very simple. Click download all to get all the compressed files at once, grouped in a zip archive. Bek a study of the dependence of nanoindentation pileup. Sep 12, 2019 an investigation of nanomechanical properties of materials using nanoindentation and artificial neural network skip to main content thank you for visiting. Fem simulation of nanoindentation applied nanoindentation.
Determination of mechanical properties by nanoindentation independently of indentation depth measurement. Pileup and sink in material behaviour at maximum indentation depth a side. These effects are not considered by the oliver and pharr method. Select up to 20 pdf files from your computer or drag them to the drop area. Van vliet massachusetts institute of technology, cambridge, ma 029, usa abstract recent progress in experimental and theoretical nanomechanics opens new venues in materials science for. For analysis of the indentation face, multiaxis flip stages are on the market that rotate the sample after indentation, further extending the possibilities of correlative afmsem. Knowledge of the true hardness of the film can be used to assess the effects of the elastic modulus mismatch on the nanoindentation properties, by using the measured contact stiffness as a function of depth of indentation relative to the. Bek a study of the dependence of nanoindentation pileup patterns on the indentation load and crystallographic orientation is presented.
Wait for the upload and compression processes to complete. Pile up correction of mechanical characteristics is based on ratio of pile up height and contact depth. Microstructures and nanoindentation behaviors were studied on annealed alcocrfeni high entropy alloy. Experimental tests have been conducted on nanocrystalline nc, ultrafinegrained ufg, and. Investigation of the mechanical properties of thin films by. Both pileup and sink in characteristics were found in the grain boundary and grain regions, respectively.
This knowledge is of considerable importance for nanoindentation testing because the shape of the outofplane displacement zone determines the actual contact area between the indenter and the specimen. Interests and limitations of nanoindentation for bulk multiphase material identification. A very important question is whether the deformations will be only delayedreversible, or if also irreversible creep will be present. Hardness hardness is a measure of a materials resistance to surface penetration by an indenter with a force applied to it. Materials with large yield strengthtoyoungs modulus ratio, ye, are likely to show sink in upon nanoindentation loading, while materials with small ye can show either sink.
Most nanoindentation analysis methods assume that surface pileup or sinkin plays a negligible role in determining contact area for the calculation of hardness. Gaylord guillonneau, guillaume kermouche, sandrine bec, jeanluc loubet. Youngs modulus and hardness data obtained from nanoindentation are commonly affected by phenomena like pile up or sink in, when elasticplastic materials are tested. These differences in the surface deformation mode affect the quantitative analysis of the hardness measurements. The oliver and pharr method however is not efficent eneough when pile up or sink. Substrate effect and nanoindentation fracture toughness. Depth dependence of nanoindentation pileup patterns in. Pdf orientation dependence of nanoindentation pileup.
Pile up height was measured by atomic force microscopy afm. For the proposed ecm, it is assumed that the volume of material displaced by the indenter is equal to the volume loss, due to elastic deformation, in the material and depends on the pileup or sink in. Apr 29, 2019 nanoindentation of three metastable dualphase high entropy alloys heas was performed to obtain their inherent elastoplastic deformation responses. Hardness brinell, 10 mm indenter, 3000 kg load f surface area of indentation a vickers, diamond pyramid indentation microhardness vickers microindentation. Pileupsinkin of ratesensitive nanoindentation creeping solids. Understanding nanoindentation unloading curves journal.